Technical FAQ

Grade selection, test methods, troubleshooting and compliance for Vistasilica precipitated silica — answered against the published specification, not in general terms. Every figure below matches the grade specification table.

Which grade fits which application

Grade selection

VS-C200 Carrier is the starting point for feed premix carrying. VS-C200 has a BET surface area of 170–230 m²/g and DOP oil absorption of 240–290 g/100 g (ISO 4652), which supports converting liquid additives and vitamin or trace-mineral blends into a free-flowing powder. Where the problem is discharge and bridging rather than liquid loading, VS-F120 Flow Aid is the closer match.
VS-C200 and VS-F120 differ in surface area, oil absorption and particle size. VS-C200 carries liquid: BET 170–230 m²/g, DOP 240–290 g/100 g, D50 10–18 µm. VS-F120 keeps powder moving: BET 100–150 m²/g, DOP 180–230 g/100 g, D50 5–12 µm, with 45 µm sieve residue ≤ 0.05% (ISO 2591-1). Use VS-C200 to turn a liquid into a powder, VS-F120 to keep an existing powder free-flowing.
VS-WG180 WG Carrier is the agrochemical grade. VS-WG180 is specified at BET 160–210 m²/g, DOP 200–250 g/100 g and D50 12–22 µm, which balances active loading against the disintegration a WG needs. Vistasilica supplies the inert carrier only and works with locally licensed formulators.
VS-OE550 Adsorbent is the edible-oil refining grade. VS-OE550 differs from the powder grades in pore structure and density: BET 400–600 m²/g, poured bulk density 350–500 g/L and pH 4.0–6.5 in 5% aqueous suspension (ISO 6588). The higher surface area targets phospholipid and soap adsorption, with filter-aid behaviour that reduces filtration load.
Ordinary precipitated silica has no meaningful affinity for fluoride ions, because its surface chemistry is not suited to that exchange. VS-DA300 is a functionalised adsorbent rather than a conventional precipitated-silica grade: a precipitated-silica framework of ≥ 70% SiO₂·nH₂O carries 8–15% supported alumina or boehmite as Al₂O₃, and those alumina surface hydroxyls are the sites that exchange with fluoride.
How the published specifications are measured

Parameters and test methods

Every parameter on the Vistasilica grade table carries its test method. BET surface area follows ISO 9277 / DIN 66131; DOP oil absorption follows ISO 4652 / DIN 53617; particle size D50 follows ISO 13320 by laser diffraction; sieve residue follows ISO 2591-1; poured and tapped density follow ISO 60 and ISO 697; pH follows ISO 6588; loss on drying follows ISO 787-2; loss on ignition follows ISO 6798.
Oil absorption measures how much liquid a carrier holds before the powder stops flowing, which is the property that decides whether a liquid additive can be converted into a free-flowing powder. Surface area describes the pore structure available for that uptake but does not translate directly into carrying capacity. VS-C200 is specified at DOP 240–290 g/100 g (ISO 4652) for this reason.
SiO₂ content on a dry basis is ≥ 97.0% for VS-C200, ≥ 98.0% for VS-F120, ≥ 96.0% for VS-WG180 and ≥ 98.0% for VS-OE550, determined gravimetrically or by XRF. Loss on ignition at 1000 °C (ISO 6798) is ≤ 6.0%, ≤ 5.0%, ≤ 7.0% and ≤ 10.0% respectively.
Dosage is set by trial rather than by a single published figure, because the working load depends on the liquid or active being carried, the mixer and the target storage condition. Vistasilica supplies a main sample together with a comparison sample around the metrics you name, so a trial can bracket the range. The dimension to measure differs by track: absorption capacity for carriers, bridging and storage set for anti-caking, disintegration time for WG.
Published industry literature reports typical loading ranges rather than a single figure, and these are starting points for a trial — not Vistasilica specifications. For anti-caking and flow in feed premixes and dry blends, hydrophilic precipitated silica is commonly reported at 0.5–2%, and EU rules cap silica at 2% of total feed. Used as a liquid carrier, the finished absorbate is commonly 30–50% silica. In agrochemical solid formulations, active loading on a porous carrier is commonly reported at 30–60% by weight. In edible-oil refining, published work reports silica adsorbent dosages from about 0.1% w/w for soap removal up to about 1.5% w/w for degumming. Confirm any of these against your own system before scaling.
The published static capacity for VS-DA300 was measured at 2 g/L, 25 ± 2 °C, 24 h contact and pH 6.5 — a laboratory test condition, not an operating recommendation. Peer-reviewed studies of alumina-based fluoride adsorbents report working doses of roughly 6–16 g/L, varying with pH, initial fluoride concentration and competing ions. The operating dose for a specific water should come from a jar test followed by a dynamic column trial.
What to check when performance does not match the trial

Application troubleshooting

Anti-caking performance depends on the moisture and fat profile of the host powder, not on the silica alone. A blend that forms recrystallised salt bridges during storage needs a different particle size and surface area from one that cakes through fat migration. Screening the powder profile before selecting a loading is what separates the two cases.
Silo caking after weeks of storage usually points to moisture cycling rather than to insufficient anti-caking dosage. Check the temperature swing across the silo wall, the loss on drying of the incoming powder, and whether the flow aid was added before or after the liquid stage. Raising dosage alone rarely resolves anti-caking, flowability and dispersion uniformity together — the Vistasilica validation guide measures the three separately.
Disintegration failure after a carrier change usually traces to the balance between active loading and pore structure: a carrier that accepts more active can also hold the granule together longer. VS-WG180 is specified at DOP 200–250 g/100 g and D50 12–22 µm to keep loading and disintegration in a workable range. Disintegration time should be re-measured whenever active loading changes.
Residual phosphorus is lowered by shifting part of the load from bleaching earth onto a silica adsorbent in the pretreatment stage. VS-OE550 targets phospholipid and soap adsorption ahead of bleaching, which reduces the earth dosage needed to reach the same phosphorus target. Four dimensions should be measured together: residual phosphorus, soap residue, filtration pressure drop and total earth consumption.
VS-DA300 capacity, operating window and service life

Industrial fluoride removal

VS-DA300 has a saturated static capacity of ≥ 20 mg F⁻/g by the Langmuir monolayer model, with R² ≥ 0.95. Measured at 25 ± 2 °C, 2 g/L dosage, 24 h contact and pH 6.5, equilibrium capacity is 2.6 mg/g at 5 mg/L initial fluoride (95% removal), 9.4 mg/g at 20 mg/L (84%) and 22.0 mg/g at 100 mg/L (55%).
VS-DA300 performs best between pH 5 and 7, which matches typical polishing-stage conditions. The usable range is pH 4–8.5, where at least 80% of capacity is retained. Above pH 9 capacity drops markedly, so front-end pH adjustment is recommended.
Sulphate, chloride and nitrate have only a minor effect on VS-DA300. Bicarbonate and carbonate compete for the same sites, so high-alkalinity water needs pH pre-adjustment or a higher dosage. Phosphate competes strongly and should be assessed before the bed is sized.
VS-DA300 is regenerated by soaking in 4% NaOH for 2–4 hours, rinsing to neutral, activating in 5% HCl for 1–2 hours and rinsing to neutral again. Capacity retention is ≥ 85% after 20 regeneration cycles and ≥ 75% after 50 cycles. Typical replacement interval is 1–2 years, depending on water chemistry and throughput.
Fluoride adsorption is a polishing step, not a primary removal stage. VS-DA300 is applied after front-end precipitation has taken out the bulk of the fluoride load, to bring the residual below the discharge limit. Asking an adsorbent to carry the full load shortens bed life and raises cost per cubic metre treated.
Registrations, approvals and the document set

Compliance and documentation

Precipitated silica supplied by Vistasilica is registered under EINECS 231-545-4 (silicic acid). The material is not classified as hazardous under CLP Regulation (EC) No 1272/2008, and it is not a nanomaterial as defined by EU 2015/2283.
Food-grade grades correspond to E 551 under Regulation (EU) No 231/2012 and to 21 CFR § 172.480 in the United States. Both apply to food-grade grades only — industrial and agrochemical grades are not supplied against these specifications. Kosher and Halal certificates are available on request for food-grade grades.
Precipitated silicic acid is listed in the EU Register of Feed Materials, which covers carrier and anti-caking use in feed premixes. Use declarations for the specific application are provided as part of the document set.
Typical maxima for food and feed grade are lead ≤ 5 mg/kg, arsenic ≤ 3 mg/kg, cadmium ≤ 1 mg/kg, mercury ≤ 1 mg/kg, and total heavy metals as lead ≤ 10 mg/kg. Reference limits are FCC and EU 231/2012 for lead, arsenic and mercury, FCC for total heavy metals, and industry standard for cadmium.
COA, SDS/MSDS, specification sheets, use declarations and required third-party test reports are supplied as a set, for internal evaluation and for the import process. A COA is also included with samples.
Sampling, minimum quantities, packaging and supply model

Samples, ordering and logistics

Samples are dispatched within 1–3 working days by air after a sample request. Vistasilica provides a main sample together with a comparison sample around the metrics you name, with a COA included.
Minimum order quantity varies by track. Formulation plants and blenders typically start at 200 kg–1 tonne with several grades in parallel; fluoride-removal trials can start at 25 kg for jar tests and comparison samples; industrial refineries and formulators usually run 1–5 tonne trial orders. Consolidation across grades is supported.
Packaging is 20 kg and 25 kg 3-ply kraft paper bags with an inner PE liner for standard export, palletised and stretch-wrapped. Bulk industrial shipments use 500 kg or 1,000 kg FIBC big bags, Type C or D, with a PE inner liner.
Vistasilica is a silica solutions brand under Vista, operated by Longyan Vista Chemical Co., Ltd. The model integrates supply with application support across the tracks — grade selection by scenario, fast sampling and repeat-order conversion — rather than quotation alone.
Vistasilica does not replicate brand premiums. Entry is through niche applications, second-source and backup supply, several grades in parallel and localised application review, which lowers trial cost for small and mid-sized plants. Brand names referenced remain the property of their respective owners.
No. The agrochemical track serves locally licensed formulators only, supplying inert carrier and rheology or anti-caking function. Active ingredients, efficacy and registration responsibility remain with the formulator.

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